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17,1926 (1978). D. J . Reynolds, Advances in Fluorine Chemistry, Vol. 7, Butterworths, London, 1973, pp. 1-68. 5 . A. J. Edwards and F. J. Hewaidy, J. Chem. SOC. ( A ) , 1968,2977. 6. S . H. Martin, R. R. Ryan, and C. B. Asprey,Inorg. , 9,2100 (1970), A. J. Edwards and M. A. Monty,& Chem. SOC. (A), 1969,703. 8. SULFUR TETRAFLUORIDE OXIDE Submitted by KONRAD SEPPELT* Checked by F. TANZELLA and NEIL B A R T L E m Sulfur tetrafluoride oxide is the only stable sulfur fluoride or sulfur fluoride oxide that is not commercially available, although its value is increasing in synthetic chemistry.
Vetsch,J. , 18,283 (1976). 8 . F. Hulliger, M. Landolt, and H. Vetsch,J. , 18,307 (1976). 9. H. Grhicher, R. Kind, W. M. Meier, and W. Petter, Helv. Phys. Acra, 41,843 (1968). 10. J. Petzelt, J . Roos, and H. Grhicher, Ferroelectrics, 13,437 (1976). 11. J . Roos, R. Kind, and J. Petzelt,Z. , B24,99 (1976). 12. F. Herlach. D. Aboav, H. Grtinicher, and W. Petter, Helv. Phys. Acra, 30,252 (1957). 13. K. Tichf, J . Bene's, H. Arend, and A. Riiegg, Report AFSSP-93, Institut f i i Reaktortechnik ETH, Wiirenlingen, 1975, p.
E. Sherry for obtaining the X-ray powder patterns. The infrared studies were performed by Dr. J. Ferraro of Argonne National Laboratory. J. M. Williams, A. J. Schultz, and R. Besinger, work in progress. 1. A. J. Schultz, C. C. Coffey, G. C. Lee, and J. 2. 3. 4. 5. 6. 7. 8. 9. 10. 11. 12. 13. 14. The Partially Oxidized Rb'(or Cs2)[Pt(CN)4/ (FHF)4 23 6. THE RUBIDIUM-CESIUM PARTIALLY OXIDIZED TETRACYANOPLATINATE (HYDROGEN DIFLUOR1DE)-FLUORIDE SYSTEMS* The partially oxidized tetracyanoplatinate (POTCP) salts continue to be of high interest because of their anisotropic metallic properties.