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By J. Hellerbach
The duty of manufacturing this e-book could were very unlikely with out support from my acquaintances and collaborators of the departments of natural Chemistry, analytical Chemistry and Pharmacology.
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Extra resources for Synthetic Analgesics. Morphinans
Example text
Ref. 6-dehydro CH3O 6 z! 6-dehydro-10,l 6-dioxo 167-170° C 1 8 H 1 9 O3N dl 173 CH3O 6,7-dimethyl-zl 6 - d e h y d r o - l 0,16- 179-181° C 2 0 H 2 3 O3N dl 173 base 184-186° C 1 9 H 2 5 ON m 173 iodo- 217-219° C 2 0 H 2 8 ONI dl 173 dl dioxo CO HO 6,7-dimethyl-zl6-dehydro HO 6,7-dimethyl-zJ 164-166° 6 -dehydro methylate HO base 217-218° C 1 7 H 2 3 ON HO iodo- 224-225° C 1 8 H 2 6 ONI methylate t Stiong analgesic activity * W e a k or n o analgesic activity > \ ) s s e . Pharmacological part. p.
The further increased activity of in use. its which skeleton. related to the two antipodes does not lend This incemizing the unwanted step of the prompted itself t o us to 3-hydroxy-JV- racemization investigate antipode at a n earlier of the owing to ( 1 5 6 ) a technically satisfactory solution of this p r o b l e m was evolved. By heating optically l-benzyl-2-methyl-l,2,3,4,5,6,7,8-octahydroisoquinolines sence of a specially prepared palladium-zinc-iron ( 1 5 7 ) or cobalt-copper are molecule but m a y SA.
P. Formula Ref. p. H6O6 C18H25ON • HBr C18H25ON C18H25ON-C4H6O6 C18H25ON • HBr Ci8H25O2N • HBr C19H27ON • H3PO4 C19H27ON • H3PO4 C20H29ON • QH 6 O 6 C20H29ON • C4H6O6 C20H28ON-HBr Ref. p. o2 173° 115-117° 160-161° 155-156° 106-108° 116° 144-145° 173-174° 224-225° 218-219° oil Formula C20H28ON-HBr C23H36ON2 C19H25O2N • C4H6 C19H25O2N • HBr C20H27O2N • C4H6O6 C20H27O2N • C4H6O6 C33H53O2N • C4H6O6 C33H53O2N • C4H6O6 C24H27O2N • C 4 H 6 0 6 C24H27O2N • C4H6O6 C24H27O2N • HBr C20H28O2N2 Ref. p. ,P* dl9 a dl, a — 69, af + 71, a -62-2, af + 60-8, a dl* -142* 2 (-) + 140 -18 + 18 + 14 -14 Ref.